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KMID : 1171820070220040065
Journal of Environmental and Sanitary Engineering
2007 Volume.22 No. 4 p.65 ~ p.76
Quantitative Analysis of Acid Value, Iodine Value and Fatty Acids Content in Vegetable Oils by NIRS
Kim Jae-Kwan

Choi Ok-Kyung
Hwang Sun-Il
Jeong Jin-A
Kim Yun-Sung
Park Shin-Hee
Son Mi-Hui
Kwon Hye-Jung
Lee Jung-Bok
Kim Jong-Chan
Abstract
The possibility of rapid quantitative analysis of AV(Acid Value), ¥³(Iodine Value) and fatty acids in vegetable oils with NIRS(Near-infrared spectroscopy) was evaluated. A calibration equation calculated by MPLS regression technique was developed and correlation coefficient of determination for AV, ¥³, C16:0, C16:0, C16:1, C16:2, C16:6, and C20:0 content were 0.9727, 0.997, 0.9805, 0.942, 0.9987, 0.9994, 0.9966, and 0.975 respectively. According to the data obtained from validation study, R©÷ of contents of perilla, corn, soybean, rapaseed oils were 0.897, 0.993, 0.935, 0.707, 0.994, 0.996, 0.984, 0.798, SEP of contents of 0.185, 1.367, 0.899, 0.640, 1.498, 1.360, 0.476, 0.076 by MPLS. The results indicate that the NIRS procedure can potentially be used as a non-destructive analysis method for the rapid and simple measurement of AV, ¥³ and fatty acids in vegetable oils.
KEYWORD
NIRS, Vegetable oils, AV, ¥³, Fatty acids
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